Quality Control Requirements Index (QC-REQ-IDX)

Document Type: QMS-Level Governance Index (L1)
Owner: Quality Control Operations (QCO) – Quality Assurance
Applies To: All GMP-relevant activities governed under 21 CFR Part 111

1. Purpose

This document establishes the Quality Control Requirements Index (QC-REQ-IDX) as the authoritative, QMS-level source of QC rules, acceptance criteria, limits, and decision thresholds governing GMP-relevant activities.

The requirements defined in this index constitute the formal QC rules under which product, material, process, facility, and data quality decisions are made. These rules are established and approved by Quality Control Operations (QCO) and are executed within the Quality Management System (QMS).

QC requirements may be executed by trained personnel performing the activity, including operators, technicians, and analysts, provided that acceptance criteria and decision thresholds are predefined, documented, and controlled. Organizational independence is not required for execution of QC requirements.

Independence is applied at the level of review, evaluation, escalation, and disposition, in accordance with the QMS. Results that meet acceptance criteria may proceed as defined, while results that exceed, violate, or trend toward defined limits require escalation and Quality Event handling per QMS procedures executed by Quality Assurance (QA).

This index enables any QC decision made during operations to be directly traceable to an explicit, approved requirement. If a quality-related decision cannot be mapped to a requirement within this index, that decision is considered uncontrolled and the requirement must be formally defined by QCO prior to system lock under the QMS.

Acceptance criteria, limits, specifications, and decision thresholds governing GMP-relevant activities are defined directly within this document where practical. Standalone specification documents that previously contained only restated limits may be consolidated into this index to establish a single authoritative source and reduce reconciliation risk.

2. Structure of Quality Control Requirements

Quality Control Requirements (QC-REQ) are intentionally divided into two distinct classes to preserve clarity of ownership, appropriate change control, and inspection readiness:

3. Product-Specific Quality Control Requirements

Product-Specific QC-REQ define what quality attributes must be met for an individual product. These requirements are approved and controlled by QCO and are implemented through QA-approved Product Specifications maintained under product-level change control.

QC-REQ Category Requirement Type Authoritative Source Document
Finished product identityRelease acceptance criteriaFinished Product Specification (Capsule)
Finished product strengthDeclared ingredient limitsFinished Product Specification (Capsule)
Finished product purityContaminant limitsFinished Product Specification (Capsule)
Finished product compositionFormula & excipient constraintsFinished Product Specification (Capsule)
Physical / appearanceVisual & physical acceptance criteriaFinished Product Specification (Capsule)
Packaging configurationSuitability & acceptance criteriaFinished Product Specification (Capsule)
Labeling (QC-relevant)Content & claim constraintsFinished Product Specification (Capsule)
Storage & handlingTemperature & RH limitsFinished Product Specification (Capsule)
StabilityShelf-life criteriaFinished Product Specification (Capsule) + Stability Protocols

4. System-Level Quality Control Requirements

System-Level QC-REQ apply uniformly across products and define Quality Control governance, authority, escalation, and decision-making rules. These requirements are owned and approved by QCO and maintained under system-level change control.

A. Environmental & Facility Control Requirements

Linked specification documents are retained for historical reference only. Acceptance criteria and governance requirements are authoritative as defined within this index.

QC-REQ ID QC-REQ Category Requirement Type
QC-ENV-001 Warehouse environmental conditions Temperature and relative humidity acceptance criteria governing GMP-designated warehouse storage areas:
  • Temperature: 55–77 °F
  • Relative Humidity: ≤60%
Approved QC acceptance limits governing storage suitability
QC-ENV-002 Production environmental conditions Temperature and relative humidity acceptance criteria governing GMP-designated production and packaging areas:
  • Temperature: 65–75 °F
  • Relative Humidity:
    • ≤60% RH for standard operations
    • ≤50% RH where required by material or product-specific specifications
Product- or material-specific environmental requirements are defined in applicable Product Specifications, Batch Records, or Packaging Instructions.
QC-ENV-003 Packaging environmental conditions Temperature and relative humidity acceptance criteria governing GMP-designated production and packaging areas:
  • Temperature: 65–75 °F
  • Relative Humidity:
    • ≤60% RH for standard operations
    • ≤50% RH where required by material or product-specific specifications
Product- or material-specific environmental requirements are defined in applicable Product Specifications, Batch Records, or Packaging Instructions.
QC-ENV-004 Temperature-controlled storage Acceptance criteria governing refrigerated, frozen, or otherwise temperature-controlled GMP storage conditions:
  • Refrigerated storage: 36–46 °F
  • Frozen storage: −4 °F ±9 °F unless otherwise specified
  • Controlled room temperature: 68–77 °F with allowable excursions per USP <659>
Product-specific storage requirements supersede system-level limits where defined.
QC-ENV-005 Retained sample storage Environmental acceptance criteria governing retained sample storage conditions:
  • Temperature: 68–77 °F (controlled room temperature)
  • Allowable excursions: per USP <659>, documented and assessed
  • Relative Humidity: ≤60% RH unless otherwise specified
  • Segregation: retained samples stored separately from released inventory
Product-specific or stability protocol requirements supersede system-level limits where defined.
QC-FAC-001 GMP area classification & zoning Classification, zoning, and segregation requirements for GMP-designated facility areas
(Facility Classification & Zoning Specification)
QC-FAC-002 Facility cleanliness Acceptance criteria defining cleanliness expectations for GMP-designated facility areas
(Facility Cleanliness Acceptance Specification)
QC-FAC-003 Facility drain design & maintenance Acceptance criteria governing drain placement, slope, cleanability, trapping, odor control, pest prevention, and maintenance of drains located in GMP-designated facility areas
(Facility Drain Design & Maintenance Specification)
QC-UTIL-001 Compressed air quality Quality classification and acceptance criteria for compressed air used in GMP-relevant operations:
  • Oil: No detectable oil carryover
  • Water: Free of liquid water at point of use
  • Particulates: Controlled to prevent contamination of materials and products
  • Source: Oil-free or appropriately filtered and monitored systems
Compressed air quality requirements are risk-based and appropriate to the intended use (product contact vs. non-contact).
QC-UTIL-002 Water quality classification Quality classification and acceptance criteria for water used in GMP-relevant operations:
  • Potable water:
    • Meets local potable water standards
    • Suitable for handwashing, cleaning, and non-product-contact use
  • Purified water (where used):
    • Meets USP Purified Water specifications
    • Used where product or process contact requires higher purity
Water quality requirements are defined based on intended use; product- or process-specific requirements supersede system-level classifications.
QC-UTIL-003 Wastewater & drainage systems Governance requirements for wastewater, sewer, and drainage systems serving GMP-designated areas, including:
  • Segregation of sanitary, process, and utility drainage
  • Prevention of backflow, cross-contamination, and pest ingress
  • Drain design to support cleanability and sanitation
  • Maintenance and inspection to prevent deterioration or leakage
Detailed execution, inspection, and maintenance activities are defined in Facilities and Sanitation SOPs.
QC-UTIL-004 Backflow & cross-connection prevention Governance requirements for prevention of backflow and cross-connection between potable water, process utilities, and wastewater systems, including:
  • Installation and maintenance of appropriate backflow prevention devices
  • Use of air gaps where required to prevent contamination
  • Physical segregation of potable, process, and waste systems
  • Periodic inspection, testing, and documentation of backflow controls
Execution, inspection, and testing activities are defined in Facilities and Utility Maintenance SOPs.

B. Product & Material Quality Control Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-MAT-001 Component identity verification Acceptance criteria and decision requirements for verification of component and raw material identity prior to GMP use
(Component Identity Verification Specification)
QC-MAT-002 Component purity & contaminant acceptance Acceptance criteria governing purity, contaminant limits, and suitability of components and raw materials for GMP use
(Component Purity & Contaminant Acceptance Specification)
QC-MAT-003 Supplier qualification status impact Decision rules defining how supplier qualification and performance status impacts material acceptance and usability
(Supplier Qualification Status Impact Specification)
QC-MAT-004 Material storage & handling condition Acceptance criteria governing material condition, container integrity, segregation, and suitability during storage and handling
(Material Storage & Handling Acceptance Specification)
QC-MAT-005 Packaging component quality Acceptance criteria governing quality, suitability, and condition of packaging components prior to GMP use
(Packaging Component Quality Acceptance Specification)

C. Sampling & Acceptance Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-SAMP-001 Sampling plan governance System-level requirements defining how sampling plans are established, approved, and governed for GMP materials and products
(Sampling Plan Governance Specification)
QC-SAMP-002 Lot acceptance decision criteria Acceptance criteria and decision rules governing lot acceptance, rejection, or further evaluation based on sampling results
(Lot Acceptance Decision Specification)
QC-SAMP-003 Sampling representativeness Requirements ensuring samples collected are representative of the lot, batch, or population being evaluated
(Sampling Representativeness Specification)
QC-SAMP-004 Reduced / skip-lot sampling Conditions under which reduced, skip-lot, or alternative sampling schemes may be applied
(Reduced & Skip-Lot Sampling Specification)

D. Analytical & Measurement System Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-ANL-001 Analytical method suitability Acceptance criteria governing the suitability of analytical methods used to generate GMP-relevant test results
(Analytical Method Suitability Specification)
QC-ANL-002 Instrument & system suitability Acceptance criteria governing the suitability, readiness, and reliability of instruments and analytical systems used for GMP testing
(Instrument & System Suitability Specification)
QC-ANL-003 Measurement uncertainty impact Requirements governing how measurement uncertainty is considered when evaluating analytical results against acceptance criteria
(Measurement Uncertainty Impact Specification)
QC-ANL-004 Outsourced testing governance Governance requirements defining acceptance and control of analytical results generated by external laboratories
(Outsourced Testing Governance Specification)

E. Process Control & In-Process Control (IPC) Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-IPC-001 Critical process parameter governance Governance requirements defining identification, control, and oversight of critical process parameters impacting product quality
(Critical Process Parameter Governance Specification)
QC-IPC-002 In-process acceptance criteria Acceptance criteria governing in-process tests and evaluations used to support continued processing decisions
(In-Process Acceptance Criteria Specification)
QC-IPC-003 Process monitoring & trending Requirements governing monitoring, trending, and evaluation of process performance and variability
(Process Monitoring & Trending Specification)
QC-IPC-004 In-process deviation response Decision requirements governing response, escalation, and control of in-process deviations impacting product quality
(In-Process Deviation Response Specification)

F. Stability, Retention & Lifecycle Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-STAB-001 Stability program governance Governance requirements defining establishment, approval, and oversight of stability programs for GMP products
(Stability Program Governance Specification)
QC-STAB-002 Retained sample lifecycle Requirements governing retention, storage, use, and disposition of retained samples throughout the product lifecycle
(Retained Sample Lifecycle Specification)
QC-STAB-003 Shelf life assignment Acceptance criteria governing assignment, extension, and maintenance of product shelf life and expiry
(Shelf Life Assignment Specification)
QC-STAB-004 Lifecycle trending & review Requirements governing lifecycle review and trending of stability, complaints, and quality performance data
(Lifecycle Trending & Review Specification)

G. Disposition, Release & Rejection Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-DISP-001 Lot disposition authority Governance requirements defining authority, responsibility, and accountability for disposition decisions of GMP lots and batches
(Lot Disposition Authority Specification)
QC-DISP-002 Release decision criteria Acceptance criteria governing final release decisions for GMP products prior to distribution
(Release Decision Criteria Specification)
QC-DISP-003 Rejection & quarantine governance Requirements governing identification, segregation, and control of rejected or nonconforming materials and products
(Rejection & Quarantine Governance Specification)
QC-DISP-004 Rework & reprocessing governance Governance requirements defining evaluation, approval, and control of rework or reprocessing activities
(Rework & Reprocessing Governance Specification)
QC-DISP-005 Conditional release governance Requirements governing conditional or limited release of product under defined risk-based controls
(Conditional Release Governance Specification)
QC-DISP-006 Microbiological acceptance Acceptance criteria governing microbiological quality of finished products prior to release
(Microbiological Acceptance Specification)
QC-DISP-007 Chemical acceptance Acceptance criteria governing chemical and contaminant limits of finished products prior to release
(Chemical Acceptance Specification)
QC-DISP-008 Identity & composition acceptance Acceptance criteria governing finished product identity and composition conformance
(Finished Product Specification)
QC-DISP-009 Potency / strength acceptance Acceptance criteria governing potency or strength claims where applicable prior to product release
(Potency Acceptance Specification)

H. Data Integrity, Records & Documentation Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-DI-001 Data integrity governance Governance requirements ensuring data is attributable, legible, contemporaneous, original, and accurate throughout its lifecycle
(Data Integrity Governance Specification)
QC-DI-002 Record completeness & traceability Requirements ensuring GMP records are complete, traceable, and reconstructable from raw data to final decision
(Record Completeness & Traceability Specification)
QC-DI-003 Document control governance Governance requirements defining creation, approval, revision, distribution, and archival of controlled GMP documents
(Document Control Governance Specification)
QC-DI-004 Electronic record & system governance Governance requirements for electronic systems generating, storing, or managing GMP data and records
(Electronic Record & System Governance Specification)
QC-DI-005 Data review & approval governance Requirements governing independent review, approval, and authorization of GMP data and quality records
(Data Review & Approval Governance Specification)

I. Change Management & Continuous Improvement Requirements

QC-REQ ID QC-REQ Category Requirement Type
QC-CHG-001 Change control governance Governance requirements defining evaluation, approval, implementation, and documentation of GMP-impacting changes
(Change Control Governance Specification)
QC-CHG-002 Impact & risk assessment Requirements governing identification, evaluation, and documentation of quality, regulatory, and business risk associated with change
(Impact & Risk Assessment Specification)
QC-CHG-003 Validation & requalification governance Governance requirements defining when validation, verification, or requalification is required following change
(Validation & Requalification Governance Specification)
QC-CHG-004 Change effectiveness review Requirements governing post-implementation review to confirm changes achieved intended outcomes without adverse impact
(Change Effectiveness Review Specification)
QC-CI-001 Continuous improvement governance Governance requirements ensuring systematic identification, prioritization, and implementation of quality improvements
(Continuous Improvement Governance Specification)